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2023
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Extraction and separation of Salidroside
Salidroside (salidroside) is a light brownish red to white crystalline powder; The air is fragrant and the taste is bitter and astringent.
Source: dried roots and rhizomes of Rhodiola crenulata (Hook. f. et. Thomas.) H. Ohba, a Crassulaceae plant.
There are nearly 100 species of Rhodiola in the world, which are mainly distributed in the Himalayas, northwest Asia and Chemalbook North America. There are over 80 types in China, mostly distributed in the southwest, northwest, north China, and northeast regions. The main production areas include Jilin, Hebei, Qinghai, Xinjiang, Sichuan, Yunnan, Guizhou, Tibet, and other provinces and regions.
Preparation method: condensation of o-methyl Benzaldehyde and acetaldehyde under alkaline conditions.
Extraction and separation method of Salidroside:
The roots and rhizomes of Rhodiola rosea are crushed into coarse powder, and then extracted with 70% ethanol. The extract is separated, and ethanol is recovered under reduced pressure. The obtained concentrate is stirred evenly with equal amount of water, left standing, filtered, and repeatedly treated for three times. The filtrate is concentrated under reduced pressure, and then extracted with Petroleum ether, chloroform, ethyl acetate, and n-butanol in turn. The ethyl acetate and n-butanol parts are respectively recycled to obtain the soluble Chemicalbook agent, and the crude tyrosol and Salidroside products are obtained.
Purpose: Used as a pharmaceutical raw material; Used for content determination/identification/pharmacological experiments, etc.
Xi’an JCF Herb
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